Thermal and Tensile Mechanical Behavior of Acetic Anhydride Treated Silk Fibres

Md. Minhaz-Ul Haque; Mst. Ayesha Akther Zaman; M. H. Rahaman; M. Z. Hossain; M. Maniruzzaman

doi:doi:10.11648/j.ijmsa.20140303.16

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Thermal and Tensile Mechanical Behavior of Acetic Anhydride Treated Silk Fibres

Md. Minhaz-Ul Haque, Mst. Ayesha Akther Zaman, M. H. Rahaman, M. Z. Hossain, M. Maniruzzaman

Published in International Journal of Materials Science and Applications (Volume 3, Issue 3)

Received: 2 May 2014 Accepted: 17 May 2014 Published: 30 May 2014

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Abstract

Acylation of fibres can provide a route to have materials with better water proofing capability. In our present study, silk fibres were treated with various concentration (5, 10 and15 wt.%) of acetic anhydride aqueous solution and then thermal properties, tensile mechanical behaviour and moisture content of acetic anhydride treated silk fibres were studied. Raw silk fibres were taken as control for comparison. It was found that elastic modulus and tensile strength of silk fibres were increased with increasing acetic anhydride concentration while elongation at break was decreased with increase of acetic anhydride content in solution. Silk fibres treated with 15 wt. % of acetic anhydride solution exhibited about 141% (from 17 GPa to 41 GPa) improvement in elastic modulus. It was also found that acetic anhydride treated silk fibres displayed higher thermal resistance and lower moisture content as compared to untreated silk fibres.

Published in	International Journal of Materials Science and Applications (Volume 3, Issue 3)
DOI	10.11648/j.ijmsa.20140303.16
Page(s)	106-110
Creative Commons	This is an Open Access article, distributed under the terms of the Creative Commons Attribution 4.0 International License (http://creativecommons.org/licenses/by/4.0/), which permits unrestricted use, distribution and reproduction in any medium or format, provided the original work is properly cited.
Copyright	Copyright © The Author(s), 2014. Published by Science Publishing Group

Keywords

Acetic Anhydride Treatment, Moisture Content, Silk Fibres, Tensile Properties, Thermal Behavior

References

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APA Style

Md. Minhaz-Ul Haque, Mst. Ayesha Akther Zaman, M. H. Rahaman, M. Z. Hossain, M. Maniruzzaman. (2014). Thermal and Tensile Mechanical Behavior of Acetic Anhydride Treated Silk Fibres. International Journal of Materials Science and Applications, 3(3), 106-110. https://doi.org/10.11648/j.ijmsa.20140303.16

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ACS Style

Md. Minhaz-Ul Haque; Mst. Ayesha Akther Zaman; M. H. Rahaman; M. Z. Hossain; M. Maniruzzaman. Thermal and Tensile Mechanical Behavior of Acetic Anhydride Treated Silk Fibres. Int. J. Mater. Sci. Appl. 2014, 3(3), 106-110. doi: 10.11648/j.ijmsa.20140303.16

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AMA Style

Md. Minhaz-Ul Haque, Mst. Ayesha Akther Zaman, M. H. Rahaman, M. Z. Hossain, M. Maniruzzaman. Thermal and Tensile Mechanical Behavior of Acetic Anhydride Treated Silk Fibres. Int J Mater Sci Appl. 2014;3(3):106-110. doi: 10.11648/j.ijmsa.20140303.16

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@article{10.11648/j.ijmsa.20140303.16,
  author = {Md. Minhaz-Ul Haque and Mst. Ayesha Akther Zaman and M. H. Rahaman and M. Z. Hossain and M. Maniruzzaman},
  title = {Thermal and Tensile Mechanical Behavior of Acetic Anhydride Treated Silk Fibres},
  journal = {International Journal of Materials Science and Applications},
  volume = {3},
  number = {3},
  pages = {106-110},
  doi = {10.11648/j.ijmsa.20140303.16},
  url = {https://doi.org/10.11648/j.ijmsa.20140303.16},
  eprint = {https://article.sciencepublishinggroup.com/pdf/10.11648.j.ijmsa.20140303.16},
  abstract = {Acylation of fibres can provide a route to have materials with better water proofing capability. In our present study, silk fibres were treated with various concentration (5, 10 and15 wt.%) of acetic anhydride aqueous solution and then thermal properties, tensile mechanical behaviour and moisture content of acetic anhydride treated silk fibres were studied. Raw silk fibres were taken as control for comparison. It was found that elastic modulus and tensile strength of silk fibres were increased with increasing acetic anhydride concentration while elongation at break was decreased with increase of acetic anhydride content in solution. Silk fibres treated with 15 wt. % of acetic anhydride solution exhibited about 141% (from 17 GPa to 41 GPa) improvement in elastic modulus. It was also found that acetic anhydride treated silk fibres displayed higher thermal resistance and lower moisture content as compared to untreated silk fibres.},
 year = {2014}
}

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TY - JOUR
T1 - Thermal and Tensile Mechanical Behavior of Acetic Anhydride Treated Silk Fibres
AU - Md. Minhaz-Ul Haque
AU - Mst. Ayesha Akther Zaman
AU - M. H. Rahaman
AU - M. Z. Hossain
AU - M. Maniruzzaman
Y1 - 2014/05/30
PY - 2014
N1 - https://doi.org/10.11648/j.ijmsa.20140303.16
DO - 10.11648/j.ijmsa.20140303.16
T2 - International Journal of Materials Science and Applications
JF - International Journal of Materials Science and Applications
JO - International Journal of Materials Science and Applications
SP - 106
EP - 110
PB - Science Publishing Group
SN - 2327-2643
UR - https://doi.org/10.11648/j.ijmsa.20140303.16
AB - Acylation of fibres can provide a route to have materials with better water proofing capability. In our present study, silk fibres were treated with various concentration (5, 10 and15 wt.%) of acetic anhydride aqueous solution and then thermal properties, tensile mechanical behaviour and moisture content of acetic anhydride treated silk fibres were studied. Raw silk fibres were taken as control for comparison. It was found that elastic modulus and tensile strength of silk fibres were increased with increasing acetic anhydride concentration while elongation at break was decreased with increase of acetic anhydride content in solution. Silk fibres treated with 15 wt. % of acetic anhydride solution exhibited about 141% (from 17 GPa to 41 GPa) improvement in elastic modulus. It was also found that acetic anhydride treated silk fibres displayed higher thermal resistance and lower moisture content as compared to untreated silk fibres.
VL - 3
IS - 3
ER -

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Author Information

Md. Minhaz-Ul Haque

Dept. of Applied Chemistry and Chemical Technology, Islamic University Kushtia-7003, Bangladesh
Mst. Ayesha Akther Zaman

Dept. of Applied Chemistry and Chemical Technology, Islamic University Kushtia-7003, Bangladesh
M. H. Rahaman

Dept. of Applied Chemistry and Chemical Technology, Islamic University Kushtia-7003, Bangladesh
M. Z. Hossain

Dept. of Applied Chemistry and Chemical Technology, Islamic University Kushtia-7003, Bangladesh
M. Maniruzzaman

Dept. of Applied Chemistry and Chemical Technology, Islamic University Kushtia-7003, Bangladesh

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APA Style

Md. Minhaz-Ul Haque, Mst. Ayesha Akther Zaman, M. H. Rahaman, M. Z. Hossain, M. Maniruzzaman. (2014). Thermal and Tensile Mechanical Behavior of Acetic Anhydride Treated Silk Fibres. International Journal of Materials Science and Applications, 3(3), 106-110. https://doi.org/10.11648/j.ijmsa.20140303.16

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ACS Style

Md. Minhaz-Ul Haque; Mst. Ayesha Akther Zaman; M. H. Rahaman; M. Z. Hossain; M. Maniruzzaman. Thermal and Tensile Mechanical Behavior of Acetic Anhydride Treated Silk Fibres. Int. J. Mater. Sci. Appl. 2014, 3(3), 106-110. doi: 10.11648/j.ijmsa.20140303.16

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AMA Style

Md. Minhaz-Ul Haque, Mst. Ayesha Akther Zaman, M. H. Rahaman, M. Z. Hossain, M. Maniruzzaman. Thermal and Tensile Mechanical Behavior of Acetic Anhydride Treated Silk Fibres. Int J Mater Sci Appl. 2014;3(3):106-110. doi: 10.11648/j.ijmsa.20140303.16

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@article{10.11648/j.ijmsa.20140303.16,
  author = {Md. Minhaz-Ul Haque and Mst. Ayesha Akther Zaman and M. H. Rahaman and M. Z. Hossain and M. Maniruzzaman},
  title = {Thermal and Tensile Mechanical Behavior of Acetic Anhydride Treated Silk Fibres},
  journal = {International Journal of Materials Science and Applications},
  volume = {3},
  number = {3},
  pages = {106-110},
  doi = {10.11648/j.ijmsa.20140303.16},
  url = {https://doi.org/10.11648/j.ijmsa.20140303.16},
  eprint = {https://article.sciencepublishinggroup.com/pdf/10.11648.j.ijmsa.20140303.16},
  abstract = {Acylation of fibres can provide a route to have materials with better water proofing capability. In our present study, silk fibres were treated with various concentration (5, 10 and15 wt.%) of acetic anhydride aqueous solution and then thermal properties, tensile mechanical behaviour and moisture content of acetic anhydride treated silk fibres were studied. Raw silk fibres were taken as control for comparison. It was found that elastic modulus and tensile strength of silk fibres were increased with increasing acetic anhydride concentration while elongation at break was decreased with increase of acetic anhydride content in solution. Silk fibres treated with 15 wt. % of acetic anhydride solution exhibited about 141% (from 17 GPa to 41 GPa) improvement in elastic modulus. It was also found that acetic anhydride treated silk fibres displayed higher thermal resistance and lower moisture content as compared to untreated silk fibres.},
 year = {2014}
}

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